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TKEAT/nENT  OP  SEWAGE  BY  THE 


A.  A.  HAMAEK/^AN 


ARAOUR    INSTITUTE   OF   TECHNOLOGY 

19  2  0 


628.3 
H17 


•i-  ■<:■  •■ :  ' 


of  Tecliaoiogy 
UNIVERSITY  LIBRARIES 


AT  539 

Hammerman,  M.  A. 
Collective  data  on  the 
treatment  of  sewage  by  the 


For  Us8  In  Ukary  Only 


I  ;  V  U  in  (    (I    U  I 
[IN,  /.  I,  S 

(   (■  I  '   ,'  f   '      '  ^ 


Collective  Data  on  the  Treatment  of  Sewag,e 
by  the  Activated  Sludge  Process 


A  THESIS 


PRESENTED    BY 


Meyer  A.  Hammerinan 


TO  THE 


PRESIDENT   AND    FACULTY 

OF 

ARMOUR  INSTITUTE  OF  TECHNOLOGY 


FOR  THE   DEGREE   OF 

Bachelor  of  Science 

IN 

CIVIL  ENGINEERING 
May  1920 


ILUNOIS  INSTITUTE  OF  TECHNOLO 
PAUL  V.  GALVIN  LIBRARY 
35  WEST  33RD  STREET 
CHICAGO,  IL  60616 


[jj  DEAN  OF  ENGINEERING    STUD 


DEAN  OF  CULTURAL  STUDIES 


I.  r  (  i- 


TASLE     QdP     CClTTICvTTS 
Bibliograplij'" 

Acknowledgement 

Introduction 

Experiments  Leadin;^;  To  Dis- 

coveiy 

Early  Exijerimenta 
Experiaasnts  At  lilancliester 

Experiments   in  The  United 

States 

Llilwalkee  ExxDeriments 

The   Sludge  And  Its  Disposal 

Graphs 


page 

I' 

V 

2 

n 

5 

n 

9 

ft 

II 

ti 

I6 

n 

22 

It 

53 

^9113 


Digitized  by  tine  Internet  Arciiive 

in  2009  witii  funding  from 

CARLI:  Consortium  of  Academic  and  Researcii  Libraries  in  Illinois 


http://www.archive.org/details/collectivedataonOOhamm 


Biblioiiraploi'- 
Engineering  &  Contracting 
Engineering  <2c  Contracting 
Enginesrini;  ^  Contraotihii 
En^ineerinji  &  Contracting 
Engineering  &;  Contracting 
Engineering  &  Contracting 
■3ngin»ering  ic  Contracting, 
Eng  ine  e  ring  ?Te  vvs 
Engine erihg  ITews 
Engineering  Ivews 
Engineering  ITews 

Engineering  ITews 
Engineering  ITev/s 

"Engineering  ITews-HecoSA^ 

Engineering  Record 

Engineering  Record 

Municipal  Journal 


Oct. 

P7 

1915 

Tsc, 

1, 

19 15 

PeiD, 

2, 

1916 

liar. 

1916 

Ai^r. 

26, 

1916 

xTov . 

8, 

1916 

Jul. 

51, 

1918 

Apr. 

j^. 

19 15 

Jul. 

15. 

19 15 

Jul. 

29, 

19 15 

Pec. 

2   , 

1915 

Oct. 

12, 

19 1 6 

17ov- 

25. 

19 1 6 

ITOT  , 

I, 

19 17 

Apr. 

5, 

19 15 

Oct. 

^16, 

19 15 

Pe"b. 

10, 

19 1 6 

I  t^!k«  this  opportunity  of  expressing  m/ 
appreciation  to  Professor  John  C.  Psnn  for 
suggesting  tliis  sutject  and  to  Miss  A.  E. 
Pisher,  librarian,  whos«  assistance  in  the 
literary  was  a  jcreat  help  to  me  in  preparing 
this  thesis. 


-I- 


Introduction 
until  recently  the  medical  profession  has 
been  the  sole  guardian  of   the  public's  health. 
The   system  it  uses  is  to  prescribe  a  cure  for 

a  disease,  but  it  does  not  seek  to  prevent  it. 
The  engineering  profession  however,  lead  by  the 
sanitary  engineer,   is  supplanting  to  a  certain 
extent  the  doctor  and  his  medicine.  A   typical 
case  is  the  fall   in  the  death  rate  due   to   ty- 
phoid fever.    This  was  accoiirplished  by  sanitary 
methods  of   treating  drinking  v/ater.   Other  cases 
involve   the  disposal  or   treatment  of   sewage. 
The  best,  cheapest  and  most  efficient  method 
of  attaining  this   end  is  a  matter  of  much  dis- 
cussion.  One  method  which  has  been  devised  re- 
cently is  the   treatment  by  the   "Activated  Sludge 
process". 

The  writer  has  chosen   this  as  his   subject, 
because  of  its   infancy  and  great  future.    The 
day  will  soon  come  when   every  city  and  town 
will  have  a  sewage  disposal  plant  that  gives  a 
profit  and  is  not  a  deficit  to   the  operators. 


-31- 


Experinients  Leading;  to  Discovery. 

The  method  of  treating  seaage  'o'j   the  ac- 
tivated sluge  rjrocess  was  first  formulated 
oy  Po'<7ler  and  iiuciford,  who  were  conducting 
experiments  on  sewage  in  Lianchesterj  Eng, , 
in  1915»  They  were  investigating;  the  action 
of  an  organism  which  they  designated  as  lij , 
Thej/  found  that,  if  this  or_  anism  was  cont'.'/i':'ed 
in  sewage,  the  sevrage  was  clarified  after  6 
hours  of  aeration  and  that  the  effluent  was 
non- putrefactive.  This  sluce  -olayed  an  impor- 
tant  part  in  the  results  obtained,  as  it  was 
noticed  that  if  the  sewa^^-e  samples  were  aar..;- 
bed  continuously  for  5  weeks,  complete  nitri- 
fication '.vas  ohtained,  Twlien  more  samples  wero^ 
to  he  tested,  the  clarified  sewage  was  drawn 
off  and  the  nev/  sample  w.-..s  used  .vith  the  old 
sludge.  The  time  for  oxidation  v/as  reduced  tc 
24  hours  after  a  number  of  samples  were  clari- 
fied without  removing  the  sludge, 

T^nese  experiments  were  "brou'ht  about  in 


-S  - 


order  to  find  a  cheaijer  and  raoxe   satisfactory 
method  of  treating  sewafee.  It  was  known  that 
the  most  costly  part  of  modern  sew?.ge  works, 
including  the  ca,pital  expenditure  and  often 
the  revenue  charges,  was  the  filtration  area 
The  area  and  cost  of  filter  beds  depends  naainly, 
it  was  found,  on  the  amount  of  colloidal  matter 
present  in  the  sewage  and  much  confusion  of 
ideas  was  due  to  the  fact  that  the  ordinary 
sewage  filter,  "be  it  contact  or  trickling,  Jras 
called  upon  to  do  t'.ro  entirely  different  things 

aj  the  same  time^for  it  to  oxidise,  granulate 
ar.d  finally  discharge  as  humus  the  colloidal 
uatters  present  and  second  to  oiidize  and  nit- 
rify substances  in  true  solution.  It  w-s  also 
rhovm  that  a  tank  effluent,  well  clarified  Tpy 
sedimentation  could,  by  accurate  distribution 
be  very  efficiently  purified  on  filters  of  fin^; 

;ra,terial,  but  even  then  the  area  and  cost  in- 
Ijolved  in  exceptionally  large  works,  made  the 
problem  a  verv  serious  one.' 


-4- 


For  these  and  of.-.er  Tez.zons   the  thoughte 
of  niany  v.'-orlcers  in  serrar:e  treatment  ivere  turned 

to  the  poEsitility  of  a  more  efficient  re- 
i"oval  of  the  collodial  matter  before  the  fi3^ 
tration  process. 

Sefore  this  process  was  evolved  ^only  pr:;x- 
tical  method  was  oy  heavj'  chemical  precipit:a- 
tion.  The  cost  cf  operating  a  plant  vThere'by 
the  collodial  matter  was  removed  "by  the  addi- 
tion of  a  chemical  to  the  sewage  was  very  hi  _;.h 
and  was  money  thrown  a^vay.  It  '^as  not  only  t'xe 
cost  of  the  enormous  quantities  of  chemdcals 
necessary,  hut  the  removal  of  the  vast  amount, 
of  resultant  sludre  that  "became  increasingly 
difficult  and  costly. 

Messrs.  Fowler  and  TJIumford  sought  to  find 
a  method  of  obtaining  a  thoroughly  clarified 
efficient  -dthout  the  use  of  large  quantities 
of  chemicals  and  with  the  minimum  production 
of  sludge.  By   a  thoroughly  cl:,rif3ed  §-iflmnV: 
is  mea.nt  one  ':frAcla   wi 3 1  not  eventually  depos- 


-5- 


solid  matter  either  on   the  "oottora  of  a  stream 
into  \f;hich  it  flows  or  in  the  interstices  cf 
a  bacterial  filter, 

Mr.  Murriford  in  the  coarse  of  research  in 
another  riutter  had  the  occasion  to  study  tlie 
the  action  of  an  organism  occuring  in  nature, 
in  pit  '.vater  impregnated  with  iron.  This  or- 
ganism-which  for  convenisnce  has  'been     desig- 
nated as  W/   is  a  true  facultative  organism, 
preferably  an  aerobe,  and  exercises  a  specific 
action  on  iron  solutions.  It  was  found  that  this 
hacillus  precipitated  ferric  hydroxide  from 
iron  solutions  and  in  order  to  precipitate  the 
iron  sufficiently  the  organism  required  a  cer- 
tain proportion  of  alhuminoid  orr.anic  matter. 
It  was  therefore  natural  that  ordinaiy  sewage 
r;hen  acted  upon  "b}'-  this  organism  could  he  util- 
ised in  this  -vaj;.  Experiments,  in  fact,  showed 
that  a  sewage  effluent  could  be  effectively 
clarified  in  this  u'-ay  when  acted  upon  by  this 
.or/;:anism  in  the  presence  of  si/w  1  Quantities 


-6- 


^,  «*>'* 


of  ferric    ycilts,    a,na  tierobic   ooriviitions  l/eiiie 
iTiaintained  in   tlie   liquid  'b;'-  means   of  a  current 
of  air.    The  process   requires   therefore   that    t'.e 
grosser  solids   should  be    removed  Toy    sedimenta- 
tion  so  ciS   to  have   the    least  a,mount   of  putre- 
factive  mt?,terials   in   the   liquid  portion  of  the 
s  6  rra^c  e  • 

The  ordinary  methods  of  sewage  analyris 
fails  to  reveal  the  change  which  has  really 
taken  t^lace  during  this  process,  as  they  do 
not  differentiate  "betv^een  organic  nitrogen- 
ous material,  in  the  colloidal  and  cr^T-stal- 
lojdal  states   respectively. 


-8- 


r.ai:ly  Experiments. 

Experiments  in  tlie  laboratoiy  were  iriide  v.-itli 
the  conditions  during  the  process  maintained  as 

far  as  possible  aerobic  throughout,  and  there 
being  always  a  certain  amount  of  ferric  liydrc.te 
j::re£ent  to  oxidize  offensive  sulfer  compounds 
o.nd  no  offensive  odor  v/as  produced. 

By  this  method  a  liiiiped  sparkling  and  non~ 
,-utrifactive  effjuent  was  obtained  from  domes- 
tic sev/age  dravvTi  from  a  sewer  near  the  labora- 
toiy,  Experiments  indicated  that  one  gram  of 
iron- salt  per  f-allcn  ^as  the  maximum  need  and 
that  a  total  of  twelve  hours  tankage,  i.e.  six 
liours  aeration  and  six  hours  settlement,  was 
sufficient. 

Another  feature  found  out  w-s  that  once  the 
;  ro'wth  of  or.r-anisms  liad  been  established  in  tJie 
tank,  there  appeared  no  difficulty  in  maintain- 
ing it.  The  one  hindering  feature  however,  was 
file  cost  of  air  blast;  the  pressure  of  air  ho'.7- 
ever,  depended  eimply  on  the  dejjth  of  •iV:^ter  to 


-9- 


Toe  Tolown  through  and  a  numliex   of   ,  _  '  ^-'eerin-- 
conditions  ^vould  naturally  affect  part  of  'lis 
protlem. 

The  advance  claimedj is  the  use  of  a  spe- 
cific orgciinism  found  in  nature,  together 
with  iron  salts,  to  affect  the  clj^rif icaticn 
of  the  effluent,  that  is,  the  coagulation  of 
the  colloidal  nritter  as  distinct  from  the  .ur- 
ifi cation  of  the  effluent  taken  an  a  whole.  To 
use  a  simple  illustration  the  addition  of  . 
little  rennet  does  not  appreciahHy  alter  t^ie 
contents  of  milk  as  a  whole,  "but  separates  it 
into  a  solid  and  liquid  portion.  The  endeavor 
of  tlie  discoverers  was  to  obtain  a  similar  re- 
sult in  the  case  of  seva-e  tank  effluent. 


-10- 


Experiments  at  Llanchester. 
Purther  experdnients  were  carried  out  on 
this  line  "by  Messrs.  Arden  cz   Lockett  in  1914- 
at  jvlancli ester.  Tlie  sanTnles  consisted  of  80  oz, 
cottles  of  I'ilanchester  raw  sewage.  They  were  a.^r- 
-vted  until  complete  nitrification,  h\''  dra^;ing 
_,ir  through  the  sewage  "by  means  of  an  orddnar;/ 
filter  pump.  For  the  first  sample  five  weeks   -:s 
required  for  com";lete  nitricication,  after  •"  '.ch 
t]'ie  clear  liquid  was  dravv-n  off  and  another  s:;.  ^le 
of  80  oz.  added  to  the  bottle  containing  the  set- 
tled sludge  and  this  again  aerated  until  complete 
nitrification.  This  method  of  treatment  vras  re- 
peated severa]  times  .vith  retention  in  each  c,:.i-ie 
of  the  deriosited  solids. 

It  w-s  found  that  the  amount  of  solids  in- 
creased and  the  time  required  for  each  success- 
ive aerating-  deminished  until  it  ivas  possihle 
to  oxidize  a  fresh  sample  within  twenty- four 

:ars.  The  experimenters  ca.]  led  these  deposited 
r^clids  ""ictivatea  sj-uogei* 


-II- 


\^ith  tliisc  activated  siud;"e  a  further  se- 
ries of  samples  '^ere  tested.  In  general  a  pro- 
vortion  of  one  Tolurne  of  activated  sludge  to 
four  volumes  of  s enrage  of  tiie  ■jreceeding  ex- 
periment much  smaller  proportions  were  used. 

rrom  these  tests  the  following.-  conclu3i(r;i3 
■vere  ms.de,  tha-t  an  extraordinary  high  degree 
of  x->urif ication  can  "os  obtained  ;vithin  a  rei'- 
sonahle  period  of  time  by  aeration  in  contact 
'.vith  the  activated  sludge.  The  amount  of  ni-. 
trificition  dependih;^;  to  a  certain  extent  on 
the  concentration  or  strength  of  the  sewage 
dealt  with.  On  the  averajje,  aeration  under  tlte 
conditions  of  the  experiment  for  a  period  of 

ix  hours,  with  subsequent  settlement,  was  suf- 
-"icient  to  obtain  a  high  percenta£;e  of  pmri- 
fication.  In  all  cases  the  resultant  effluent 
"as  non-putrefactive  on  incubation.  . 

These  experiments  were  'vorked  on  the  dra- 
md  fill  method  and.  it  'vas  anticipated  that 
equally  f-ood  results  could  be  obtained  by  vvor^li- 
in.^  on  a  continuous  flow  basis. 

-12- 


Further  experiments  in  tiiis  line  showed 
that  the  activity  of  the  sludge  is  gradually 
diminished,  when  working  on  the  fill  and  draw 
method,  if  it  is  called  upon  to  treat  futher 
samples  of  crude  sewage,  prior  to  the  complete 
nitrification  of  the  previous  samples  dealt  with. 
The  results  also  showed  that  this  difficulty 
would  be  overcome  by  simple  aeration  of  the 
sludge  alone,  until  the  free  or  saline  ammonia 
content  was  removed. 

Experiments  were  then  carried  on  to  deter- 
mine the  influence  of  temperature  on  the  oxida- 
tion, prom  these  experiments  it  was  found  that 
the  oxidation  process  could  be  maintained  with- 
in a  fairly  wide  range  of  temperature.  The  ex- 
periments carried  on  for  temperature  less  than 
10  C  showed  that  an  inactive  sludge  was  produced. 
With  a  temperature  of  30°C  it  was  found  that  the 
initial  clarification  effect  was  to  some  extent 
interfered  with  and  that  the  effluent  resulting 
from  subsequent  settlement  showed  a  slight  deter- 
ioration, , 


-13- 


Activated   sludge  aocumulated  in  this  raadAer 
as  descri'bed  'oy   the   investisators  is   "quite 
inoffensive,    dark  Taown  in  color,   and  flocculent 
in  character,    and   despite   its  low  specific   grav- 
ity separates   from  v;ater   or   sewage  at  a  rapid 
rate.    After   prolonged  settlement    the    activated 
sludge,  however,   rarely  contains  less   than  95 
per  cent,    of  water,   A  remarkahle   separation  of 
the  water  from  the   sludge   can  he  readily  obtain- 
ed "by   treatment  of  find  grade   strainers,  with 
the  production  of  a  sludge   of   the  consistancy 
of  a   stiff  jelly.    Gelatine  counts  have   shown  a 
bacterial  content  of  at  least   thirty  million  or- 
ganisms per  cubic   centimeter.    In  addition,    the 
sludge,  hy  reason  of  its  nitrifying  power,  must 
of  necessity  contain  a  large   numher  of  nit±lfy- 
ing  organisms.   It   should  also  "be  noted  that  a 
fairly  large  nura"ber  of  protozoa  were   found". 
It   does  not,   however,   contain  any  algae  growths. 
The  chemical  analysis  of   an   average   sample  of 
activated  sludge   is  as  follows :- 


-14- 


Organic  Katter  64.7  Per  cent 

Mineral        "  35.3      "  " 

Total  nitrogen  (n)       4.6  "    " 

Phosphate  (PS  05)        2.6  "    « 

Matter   extracted  "by 
CarlDon  Tetrachloid  CGL4  5.8     "  " 

Attention  should  'be  called  to  the  ahnorcially 
high  percentage  of  nitrogen  as  compared  with 
ordinary  unoxidised  sewage   sludge. 

Experiments  77ere  carried  out  in    the  open,    as 
compared  v;ith  the  previous  experiments  which  \7ere 
performed  in  a  laboratory  and   the   same  results   ob- 
tained.  An  air   diffuser  was  also  uded  instead  of  an 
air   tube  and   the  results    showed  and  increase  in   the 
oxidation   of  sewage.   A  continuous    system  of  flow 
was  also   tried  and  the   result  was    that   the  amount 
of  ammonia  present  in    the   effluent  increase'd  as 
the  experiment  proceeded  and  rendered  it  necessa- 
ry to  recirculate    the  effluent   through  the  aera- 
tion   tank  again.   Prom  this  it  was   seen   that    the 
sewage  must  flow  very  slowly   through  nine    series 
of  aeration   tanks  in  order    to  properly  purify 


-15- 


the  sewage, 

-■■    ■  ! 

I 

Experiments   in  U.S. 
Similar   experiments   of  this   sort  were  con- 
ducted in  America  at  Urbana,   111,    in  TsToTrem'ber 
1914  and    then  tn  a  large    scale   in  May  1915  by 
Edward  Bartow  and  5',W,Mohlman  of    the  State  Y/ater 
Survey,  University  of  Illinois,    The  first  exper- 
iments were  made  on  raw   sewage  without  activated 
sludge  present  and  the  results  showed  that  com- 
plete nitrification   could  be  obtained  within   the 
limits  of  15to33   days  by  blowing  air   into   the   sam- 
ple by  way  of  a  tube.    They    then  used  an  air   diffu- 
ser  with  a  similar   sample   of   sewage  and  complete 
nitrification  accured  within  15   days.    In  each 
case  the   faee  ammonia  nitrogen  was  oxidized  to 
nitrite  nitrogen  and  further  oxidised  to  nitrate 
nitrogen.    It   took  4830  cuft  of  air   in    the   second 
case  for   the  forsiation  of   the  nitrate.   At   the  end 
of  seven  days   the  free  ammonia  nitrogen  was  com- 
pletely changed   to  nitrite  ni tro gen , slowly  changed 
to  nitrate  nitrogen. 


-16- 


When  a  similar    sample  was  examined  in  the 
presence  of  activated   sludge  complet  nitrifica- 
tion "was  accomplished  in  five  days  and   the  amoimt 
of  air  used  "was  only  1270  cu.   ft.   The   supernatant 
liquid  was    then  drawn  off  and  another   sample   added 
to    this   accumulated  sludge   and  aeration  continued. 
In   this    treatment  complete  nitrification    took 
place  in  two   days  with   the  use  of  hut   720  cu.ft. 
of  air.    Treatments  7;ere  continued,   al-ways  de- 
canting off  the  clear   liquid  and  a  new  sample 
added  to    the   sludge  accumulated  until    the   twelfth 
treatment,  when    theresults   shov?ed  complete  nitri- 
fication in  less   than  eight  hours  with   the  use  of 
only  128  cu.    ft.    In  the   thirty-first    treatment 
there  had  already  settled  enough  sludge    that   the 
proportion  of   sewage   to    sludge  was  five  parts    to 
one  part.   Por   this  sample  purification  was  oh- 
tained  in  less   than  five  hours  using  35  cu,   ft, 
of  air,    this  heing  ahout  3   cu.ft,    per  gallon  of 
sewage, 

samples   taken  every  hour   of   the   sewage,   in 
the  operation  of   the  last  experiment  named,    showed 


-17- 


■)      -;j/ 


M  :.  n  1  I  ,  \  rr\-c  I  I  I  \ 

At  Uji   i     _ 

that    the  free   ammonia   is  not  chagged   to  nitrite 

and    the  nitrite   oxidised   to  nitrate  but    that  ni- 
trates and  nitrites  were  formed  simultaneously. 

Biological   examinations    then  made   in   the 
sludge   showed   the  presence  of  a  slender  v/orm 
whose  lenght  varied  from  two    to   five  ram.   It  is 
known    to  abound  in  fresh  water  bodies  where   there 
is  an   abundance  of  decaying  organic  matter   and 
thrtves  especially  where    there  is  much  fermen- 
tation  and  in  waters  contaminated  with  sewage 
providing   there  is  an  abundance  of  oxygen.    These 
worms  probably  destroy  at  least   their  own  weight 
of  organic  matter   each  day.   Because  of   their  re- 
production by  fission  extensive  colonies  can  be 
produced  within  a   short  period. 

These  worms,   no  doubtedly  are   the  main  con- 
tent of  activated   sludge.    The   sludge   does  not 
have  an  unpleasing  odor,    owing  to    the   fact   that 
it  consists  largely  of  living  organisms.    If  kept 
for  a  long   time   in  a  moist  condition  without  air 
i  t  will  piitfcfy.    The  chemical   analysis  of   this 
sludge   after   drying  first   on  a  water  bath,    then 
for   three  hours   in  an  oven  at  lOO^C   the  loss  of 


-18- 


t^ 


moisture  Tseing  95,54  j\er  cent»  was:- 

lTitrogen(N)  6,3  Per  cent, 

phosphorous  (p    I  1,44   "  " 

phosphate(^P^05)  3.31   ",        " 

Pat  4,00    "  " 

Volatile  matter  lost 
by  ignition  75.00   "        " 

The  percentage  of  nitrogen  and  Phosphate 
are  higher  in  this  sludge  than  that  obtained 
at  Manchester, 

Eurther   experiments  v;ere  made  at  Urbana 
in  May  1915,    These  experiments  "were   conducted 
in  four  large   concrete    tanl:s   each  having  an 
aeea  of  10   sq.ft.    and  8ft. 5in.    depth  above 
X^  in.   filtros  plates  which  were  used  to   dif- 
£use    the  air.    In    two    tanks,  hine  plates  were 
used  with  spaces   of  one    inch  betv;een    them  and 
in   the   third   tank   there  were   three  plates  cov- 
ering one- third   the  area  of   the  floor  with  a 
central  tl'ough  sloping   to   the  plates  at  an  an- 
gle  of  450, Jn  tiij  fourth  tank  one  plate  was  used 
in   the  center  covering  one  ninth  the  area  of   the 


-19- 


floor   and  7a th   the  bottom  sloping  to   it  at 
an  angle  of  45°   on  all    sides.   Below    the  plates 
was  an  air    space  of  four  inches  deep.    These    tanls 
could  "be   filled  in  six  minutes  and  drained  in 
eight  minutes,    through   two   outlets  which  are  re- 
spectively 2»   6"   and  5'    7"   alROVe  the  porous  plates. 
Uo  iludge  was  lost   through   the  outlets  of   the 
third   tank  "because  movable   outlets  were  used.    TJie 
first  and   second   tanks  were   filled  with   the   same 
kind  of   sewage,    the    sewage  in   the   first    tank  be- 
ing aerated  continuously,    and  in   the  second   tank 
for  23  hours,    the   sludge  b44ng  allowed   to   settle 
and   the   supernatant  liquid  drawn  off  and  one  hour 
later  more   sewage  added  to   the  collected   sludge. 
This   cycle  was  repeated  daily  and  results  were 
recorded.    After   ten   days  one  per   cent  of  volume 
in   the  first   tank  was   sludge   and  in   the   second 
tank  10^,    The  effluent  from  the    second  tank  was 
clearer   than  that  of  the  first    tank.    The   opera- 
tion of   the   second   tank  was  continued  as  before 
and  after  15  days, nitrification  was  complete. 


-20- 


The   sewage  was    then  changed  every   twelve  hours 
and  nitrification  was  complete  in   eight   days. 
Changing  the   sev.'age  every  six  hours   did  not   show 
good  results   and  it  "was  necessary   to   aerate  for 
longer  periods.    This  comparison  indicates,  how- 
ever,   that   sludge  may  be   satisfactorily  activa- 
ted by  changing   the   sev.'age  before  nitrification 
is  completed  and   that    the   sewage  may  be  changed 
at  frequent  intervals.    The    third   tank  give   stable 
effluents   after  five  days.    The  fourth  tank  did 
not  give   stable   effluents   in  18   days*^ 

Further   experiments  at  Jlrbana  with  activated 
sludge   took  place  in  1916  with  continuous  opera- 
tion and  results   showed    that  90^  of   the   suspended- 
matter  was  removed  and  after  13  days   of  operation 
stable  effluents  were  obtained. 


-21- 


MilwauJ^ee  Experiments, 
Further  experiments  v-ere  carried  out  "by 
T.   Challcley  Hatton*  chifif  Engineer,   llilwaukee 
Sewage  Commission  at  Milwaukee   since   1914,   The 
magnitude  of   these  experiments  Taeing  larger    than 
those   at  Urbana,   Experiments  were  carried  out 
in  liTarch  1914   one   a  small    scale   so  as   to  get  an 
idea  as  to    the  plant  necessary   to  experiment  on 
a  larger  scale,    Tww  glass    tubes  6'   long  "by  1^^' 
in   diameter  were  used.   Air  was  forced  into  one 
of  these    tubes   through  filtros  plates   and  an- 
other   through  a    tube.  Results   showed   that  after 
24  hours  aeration   in  each   tube    the  nitrification 
in  each  of   the   tubes  was  about    the  same,   A  tank 
of  Isrger  capacity  was   then  built  outside.    This 
tank  measured  32 ♦   lone  108  6"  wide  and  10 »   deep, 
piltros  plates  were    set  at    the  bottom  of    this 
tank  and  the   effluent  drawn   off  by  means  of  a 
floating  circular  weir.    This   tank  was   operated 
under   varying  conditions.    The  results   for  nor- 
mal  conditions  being,   filling  one  hour,   aerat- 
ing three  and  one-half  hours,    settling  one-half 


and  drav/ing  one  hour,   Further  experiments  were 
carried  on   in  a    tank  10  ft.   hi^  5  ft  wide,    one 
foot  between    sides.    Glass  plates  were   inserted 
at  various   depths   to   observe    the   action   inside. 
The  results  obtained   from -/this  experimental   tank 
showed  a  greater  number  of  bacteria  per  c  .c,    for 
the  filteos    tank   than  for    the  iit    . ■  Jet  diffuser 
tank.Sxperiments  were    then   conducted  on  continu- 
ous  flow   operation.    The    tank  being  of   the   same 
size  as   the   one  used  in  the   second   set  of  exper- 
iments.   This  tank  was  put  into  oeration  after 
securing  the   activated   sludge.  Experiments  were 
carried  out  with  varying  Trolumes  of  air   per  gal- 
lon of   sewage    treated,    varying  rate  of  flow  and 
varying   the  volume  of  activated  sludge.    The  re- 
sults  for    this   tank  are  as  follows,    the  larger 
percentage   of   the   sludge  in    the    tank,    the  more 
nearly  complete  nitrification  is  obtained,    that 
is, for  percentages  of    sludge  up    to  12-g^  for  vol- 
ume. 

All   of   the  preceeding   esflperiments  were  car- 


-23- 


%'.'.^' 


ried  out  in  relatively  warm  weather,    so    the 
question  came  up  as  to   hov;    the  process    .vould 
work  in  cold  weather,   as    the  "bacteria  did   their 
test  work  in   tezaperatures  between  689    to   70°P 
Tests  were  made   on  the  liilwauicee   Sewage  in  Win- 
ter  the    temperature  of   the   Sewage  ranging  from 
55°p  to   420p   and  it   occasionally  dropped  down 
to  4oO  These   ?ery  low   temperature,   re  tar ted   the 
oxidation  of    the  organic  matter   and  decreased   the 
staTaility  of  the   treated  liquid.    Activitjfng   this 
sewage  with  2^  cu,   ft.    of  air  per   gallon,   90 
per  cent   of  bacteria  in   the   se;vage  was  removed 
and  the    suspended  matter  reduced   to   about  15 
parts  per  million. 

By  increasing   the  ipolume  of  air  applied 
■  the  plants  could  remove    the   suspended  and  col- 
loidal matter  and  bacteria  in  a  satisfactory 
manner.   As   the   temperature  of  the   sewage   dropped 
the  oxidation  of    the   organic  matter   decreased 
the  nitrates  in   the   effluent  falling  more   than 
100  per  cent  for  a  difference  of    temperatures 


-24- 


of  63*^    to  49°    3-^^   the  oxygen  consumed  "was  in- 
creased 75^.   Tlie  decrease   in  oxidation  was   al- 
so  accompanied  ^by  a  decrease   in   the  stability 
of   the   effluent.    In  cold  weather    the    treated 
liquid  contained  a  large  percentage  of  dissol- 
ved o:xygen  and   only  a  trace  of  nitrate,  where- 
as in   suminer   the  nitrates  were  high  and   the  dis- 
solved o:jcygen  low.    This  shows   that   the  liquid 
seems  to   depend  upon  nitrates  in  summer   and 
dissolved  oxygen  in  winter  for   its  stability. 
This   shows  that  in  winter   temperature,    good 
"bacterial  removal   and  ci.arification  can  "be 
aiaintained  without  oxidising  the   ammonical 
nitrogen  to  nitrate. 

These,  and    the  proceeding  Kil*aukee  exper- 
iments proved   that   it  was  possible   to    treat    the 
sewage   of  Milwaukee  by  the   activated   sludge  pro- 
cess on   the  continuous  flow  method  when   the  tem^ 
perature  of   the    sewage  was   50°P  or  over  at  less 
cost   than  by  any  other  process.    It  was    then  de- 
cided   to  build  a  plant  having  a  capacity  of 
1,600,000  gallons  a  day.    The   estimated  cost  of 


-25- 


the  plant  was  ^65,000  "but   the  plant  -was  complete^ 
in  January  1916   at  a  total  cost  of  but  $61,536   in- 
cluding all  machinery  and  cost  of  engineering  and 
inspecting. 

The  activated  sludge  plant  is   Ideated  on  Jones 
Island,    alongside   a  large   outfall   sewer  of    the   com- 
bined   system.    It  consists   of  eleven  cylindrical,   so 
that  if   the   activated  sludge  process   should  fail 
they  could  be  easily  converted  into   Iichoff    tanks. 
Of   the   elven   tanks,    eight  used  in   series  are  used 
for  aeration  of  the    selvage   in    the  presence  of  ac- 
tivated sludge,   one   is  a  sedimentation    tank  and   two 
are  sludge,  aecation  tanks.   The   sise  of   the   tanks 
are  as  follows,    they  are   all  30*    in  diameter  and 
have   side  walls  extending  13 ♦    above  its  inner  bot- 
tom.   The    total  depth  of   sewage   and  sludge   is  10* 
and   the  average  depth  is  9'    in    the    ten  tanks  used 
for  aeration.    The    sewage  and   the   sludge  in   the   sed- 
imentation  tank  is  35, 2»   deep.    The  holding  capacity 
of  Aach  of   the  eight   sewage  aeration   tanks  is  45000 
gallons  or  360,000   for   the  group.    The  open  area  of 


-26- 


©  ,■ 


6ach  of   these    tanks   is   662,84   sq,  Pt,    and  all 
4f   them  5,303   sq.    ft.   The    sedimentation  tank 
has  a  holding  capacity  of  33,   000  gallons, 
not   including  2,260  gallons  held  Toy   the   48" 
cast   iron  sludge  pipe  extending  "below   its  bot- 
tom. 

The  general   scheme   of  operation  is  as 
follo"ws:    the   sewage  is   admitted   to   tank  1 
where   it  is   aerated  with  activated  sludge,   it 
then  passes    succession   through  the  first 
eight   tanks   the   combined  sewage   and   sludge 
passing  on  from  one   tank    to   another   and   then 
into    the   sedimentation   tank  9.   Here    the   sludge 
settlement   and  the  clear  liquid  passes  out  in- 
to   the  lake,   Prom  the  bottom  of   the   deep  well 
in   tank  9   the    sludge  is   discharged  by  gravity 
into   either    of   the   sludge  aeration   tanks  10  or 
11,    The  aerated   sludge   from  these   tv.'o    tanks 
passes  outside   the    tanks    to   a  48"   vertical  cast 
iron  pipe   set  28^«   in  the  ground  from  which  it 
is  lifted  by   air   and  returned  to   the  inlet   to 
the    sewage-aeration  tank  1, 


-27- 


Tlie  portion  of   the   activated  sludge   in  ex- 
cess  of  what  is  necessary   to  maintain    the  proper 
percentage   in   the  aerating  tanlca.  is  pumped  out 
of   the   sludge    tanks   from   time   to    time   and  de- 
watered  and   sold  as  fertiliser. 

The  normal  lake  level   is  at  El, -1.4.  Tlie 
sevjage  level  in   tank  1   is  El,-V    0.8   and   the 
weir  in  the   sedimentation   tank  is  at  El.  ^  0.5 
giving  a  fall  of  3»    in  water   level    through   the 
series  of   tanks. 

By  means  of   the   curved  baffle  or  division 
wall:    the   sewage    travels  and  is   subjected   to 
aeration  for  a  distance   of  912».  Air  diffusion 
affected  "by  means  of  12  x  12  in.   filtros  plates 
781n  each  sewage   and   sludge   aeration  tank.    This 
gives   a  ratio  of   diffusing  surface   to   tank  sur- 
face  of  1   to  8.5.  Tlie  filtros  plates  are   set   in 
aast   iron  frames,  which  afford  an  air  supply  con- 
duit beneath  the  center  line   of  each  plate   .   The 
estimated  air  capacity  of   the   filtros  plates  in 
the   eight   sewage   aerating  tanks  is  2  cu.    ft.   per 
minute   and  in  the   tv.'o    sludge   aeracing   tanKs   it  is 


-28- 


12  cu.it.  in  ecion  c^se  unaer  u,  2  in.  ^c^ter 
pyeseure. 

This  plant  was  designed  to  treat  1,  600,(X)0 
gallons  of  sevrsige   per  djy  with  a  four  hours  es.. 

iod  of  aeration  and  with  25  pe^:  cent  activated 
sludge  content,  a  velocity  of  3.8  '  per  min. 
and  27  min.  sedimentation  petiod.  It  can  also 
Toe  run  with  25  P^i"  cent  activated  sludge  pres- 
ent running  through  at  a  velocity  of  5  ^"t*  "02: 
5  hours  and  a  20  Eiin.  sedimentation  period,  the 
capacity  for  this  operation  "being  2,160,000  gal- 
lons, A  capacity  of  2,304,000  gallons  daily  is 
ohtained  .vith  20fS  activated  sludge  running  through 
at  a  velocity  of  5  ^t.  per  min.  for  3  hours  and 
a  $SL   19  minute  sedimentation  period. 

The  results  drawn  from  this  plant  after  a 
year  of  continuous  operation  are  numerous,  and 
man;,'-  new  experiments  were  tried  there,  but  on  a 
larger  scale,  and  their  results  obtained. 

mien  this  plant  was  first  put  into  operal^i^n 
it  required  from  30  to  55  claj'-s  of  aeration  to 
o"btain  a  sufficient  cuantity  of  activated  slud^ 


-29- 


30  as  to  start  work,  and  in  order  to  niaintain 
25  per  cent  of  activated  slud£:e  in  the  aerating 
tanks  it  had  "been  found  necessary  to  return  frora 
the  sedimentation  tank  from  40  to  ^0   per  cent  of 
the  voluire  of  raw  liquor  treated,  hecajjaea  the  Li- 
quor drav.Ti  from  the  sedimentation  tank  was  only 
about  one-half  sludge. 

Tests  for  this  best  diffusers  to  use  v;ere 
also  made.  It  was  found  that  the  filtros  diffu- 
sers created  too  much  frictional  Iobs,  the  loss 
being  three- fourths'^f or  forcing  a  five'^-air  pres- 
sure through.  Tests  v/ere  made  with  wood  block 
cut  from  basswbod  across  the  grain  and  the  fric- 
tional loss  for  these  filters  were  only  oneOhalf 
pound  for  five  pound  air  pressure.  The  wood  fil- 
tros plates  are  cheaper  and  nitrification  V7ith 
less  air  could  be  secured  by  increasing  the  dif- 
fuser  area  about  3^fo   over  air  required  for  fil- 
tros, and  thus  reducing  the  volume  of  air  pas«- 
ing  through  each  square  foot  of  diffuser. 

The  aerating  tank  which  gave  the  best  re- 


-30- 


suits  in  luilwaukee  has  the  following  proportions: 
1  sq.  ft.  of  diffusing  surface  to  5-5  sq.  ft.  of' 
tank  surface,  average  depth  of  liquor,  9  ^t.  275 
gallons  of  rav;  sewage  treated  per  day  per  sq,  ft. 
of  surface.  One  culDic  foot  of  aerating  tank  ca- 
pacity  treats  29  gallons  of  sewage  per  day. 

The  results  obtained  from  the  sedimentation 
tank  at  this  plant  were  not  very  good,  the  Elua,:e 
could  not  lina  its  wd^'-  dov/n  the  central  well  and 
therefore  collected  on  the  sloping  iDottom  of  the 
tank  and  the  sludge  became  septic.  This  settling 
in  this  manner  v;as  due  to  an  entrance  velocity 
which  -^.s  too  great  and  adverse  currents  were 
established  which  held  the  finer  flock  in  sus- 
pension, permitting  it  to  pass  over  the  wtn 
with  the  effluent;  the  heavier  sludge  v/ould 
settle  or  the  sloping  bottom  and  not  slide  down 
to  the  central  well  and  it  became  septic  there, 
Prom  further  experiments  conducted  it  was  found 
that  the  tank  giving  the  best  Sedimentation  was 
a  tank  ,7110 se  ratio  of  -^he  breath  to  the  len^JtCti 


-31- 


m^  lii^'i'w 


was  as  1  to  2.3  with  flow  across  the  breath. 
The  running  velocity  should  not  exceed  3  ft. 
horizontal  per  minute.  The  detention  period 
may  Toe  i'rom  30  to  ^0   minutes,  according  to 
the  character  of  the  selvage  treated.  Vertical- 
horizontal  flow  heing  more  efficient  than 
either  vertical  or  horizontal  flow.  The  eff3.u- 
ent  should  he  removed  with  the  least  Velocity 
Tjossihle  and  over  Continuous  rather  than  V 
shaped  weirs  the  latter  creating  cross  cur- 
rent just  where  they  are  most  ohjecitional. 


-32- 


Tlie   Sludge   and  Its  Disposal.' 
After   ti'id  sludge   ccllects   into   the    sedi- 
/iientation   tank  it    is   rei.-oved,    aevntatered,    pre-Soed 
.-nd  sold  ae   fertiliser.    The   fertilizer  "being 
^,old  for  ^12.50  per   dry   ton  in   1937,    Tlie   cost 
liowever,    of  pressing  and  di^'^ing;   the   sludge  v.-_. ich 
Included   inter^r^.t    charges  and  plant   deprecii-.tion, 
lalDor  and  iraterials   vvas  ahout.  $8.75   per  dry   ton. 
The   clear  profit  bein  ^5.75  per   ton.    An  analysis 
of   the    sludge   ohtj^ined  is  as  follows: 
Nitrogen  ^.lf=     as  1^5 

rat  5.3^ 

«    Soluble  Phos- 
phor i  c  ac  i  d       9 . 5/'V 

Potash        ,2^'ji 

The  value   of  the    sludge   depends  upon  sev- 
eral  things  among   v.-hi  oh  may   be  v/entioned  the 
percentage   of  availa'ole  nitrogen  and  the   quan- 
tity   of   fatly   liiatter   it    contains.    The    nT-;htr 
the  nitrogen  content,    the  more  vailuaV.le    is   the 
sludge   for  nianure,    but   on  the   otlaer  hand,    the 
hi^^her  the   fatly    content    the   less   &uitc*Gxpi   is 


-33- 


J- " 


ti'ie    oiuci^e   lor  agricultural   use   until    the   i.^.t- 
Ler  inateria,!  has  "been  reixoved.    Ho'vvever,    the 
rore   f-ot  present,    tlie   more   advisable    it    is   to 
i-i-eat    the    £lud:.e    to    recover    this  fat,    if  it    is 
_. resent    in   consiaera'ble   quantities, 

■Estirnating   that   one   dr;"    ton  could  he   o"b- 
tained  from  1,000,000  gallons   of   sewage   treat- 
r-d.  and  an  average    daily    dry   v;eather  flow  of 
'5><^00,000  gallons   the  nc-t   cost    of   disposing 
>!il',vaukee '  s    sewage   r/as   estiinated  at   |9.64  per 
1,000,000  j^allons   of  which  4-.  39    is   charged  to 
overheads  and  ■;4-.75   "^'^   operating,    uenewals,    and 
repairs.    The  net   cost   of  operation  per  capita 
is  figured  out   to  Ids  ,53p» 

But   this  Tfidy   not  Toe   true,    The   actual  valu-^ 
of  sludge  manure,    depends  upon  the   ease  with 
'.■/hich  it  can  "be    disposed  of.    Por  small  coiiunu- 
•-ities   surrounded  hy   rural  districts   fiere   may 
'ossilDly  no   trouTole   -.vhatever   of  disposing   of 
this   sludge   at  a  payahlo  ^.rice.    !But  v;hen  a,  rrr-i.-.t 
osnter   is   considered,    where   great   quantities   of 


-34- 


<  ( 


the  sludge  could  "be  xDroduCv...^,  .^.,^/c  is  more  t.-.an 
can  "be  used  by  tlie  surrounding  farmers^!  to  ■;  et 
rid  of  it,  uovld  have  to  "be  transported  a  £r;^at 
distance  and  sold  at  :z   cheapear  price  to  make  up 
for  're  transportation  cost.  Sewage  sludg-c,  ho-.vO 
3rer  .'   high  in  available  nitrogien  is  not  BBch  a 
rich  manure  that  it  can  stand  the  cost  of  hein^ 
carried  half  way  across  t'le  \7orld  like  the  chil~ 
ean  nitrates.  A  comparatively  small  amount  of 
handling  and  carria^-e  kills  it  as  an  article  of 
commerce. 

Activated  sludf;:e  can  he  stored  for  a  time 
oeca-use  there  is  no  offensive  oder  to  activated 
sludge,  but  considerahle  oiier  mxay  attend  impioper 
siudge  reduction.  Partially  de'.vatered  sludge,  if 
exposed  to  the  sun  for  a  few  hours  gives  off  a 
.  ighly  oh.iectional  odor  of  hydrogen  sulfate.  This 
odor  lasts  for  a  short  time  only   or  until  a  .Iiy 
cohering  is  formed.  Suldge  placed  under  cover  and 

not  exposed  to  the  sun  ::^.ives  off  little  or  no 
odor.  Flies,  insects  s,nd  '.vorms  do  not  infest  the 


-S5- 


-    ©r:*fW^, 


treatment  plant,    even   during   tlie   early   fall 
vhcn  tiiey   are   so  prevalent    in  nearly  all  otl.sr 
types   of  disposal  plants. 


-36- 


a 


!  -   '    ■' 

i     • 

i 

p--                     .,,... 

!■    ;     i    '  '■■■- 

r      ■  i 

1 
1 

Bacteria 

DuriNa 

i 

Different  Periodsiofl     i 

i                 : 

-  i—  -     . 1 

L-.-    ,■_._.  .J 

L^Aeration 

f 

T                                     I 

\ 

1 

i-   -  - 

1 

1 

j 

:  (  !         / 


/ 

/ 

t^i 

*^ 

-_ - CODE' 

9  per  ceJotAc+ivatei^ludgs 


Totat  Bacteria  per  c c— 


Hours      Aeration 


Effect;  ot  Varyinc^ 
Proportion'o  ofAdivated  5ludge 


CODE 

Curves^'-A-  lVdl.'51we(ge +o  SVol.  Sewage 

-  j|--EnJ  Veil.  Sludge  to    6 VoV.  Sewage 

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